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HRID2109463

反应详情

EQUATION

反应方程式

HRID 2109463 的结构方程式

REACTANTS

反应物

3
结构：OB(O)c1cccnc1
HCID2734378

3-Pyridinylboronic acid

C5H6BNO2

结构：Brc1coc(-c2ccncc2)c1
HCID57634253

4-(4-Bromofuran-2-yl)pyridine

C9H6BrNO

结构：C[Si](C)(C)c1oc(Br)cc1Br
HCID57634265

(3,5-Dibromofuran-2-yl)(trimethyl)silane

C7H10Br2OSi

PRODUCTS

生成物

1
结构：Brc1coc(-c2cccnc2)c1
HCID57634234

3-(4-Bromofuran-2-yl)pyridine

C9H6BrNO

PROCEDURE

实验过程

The sub-title compound was prepared by a method analogous to that described for the preparation of 4-bromo-2-(4-pyridyl)-furan from 2,4-dibromo-5-(trimethylsilyl)furan and pyridine-3-boronic acid. The sub-title compound (725 mg) was obtained as a beige solid, m/z 224,226 (MH+).

WORKUP

后处理

  1. customThe sub-title compound was prepared by a method analogous to