HuagongsheHuagongshe Chemistry Print Report · For research reference only
AR-R-17779 → HCID 57634228, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | AR-R-17779 | HCID 5310971 | — |
| Reactant | 2-Bromo-5-phenyl-1,3,4-thiadiazole | HCID 13104117 | — |
| Catalyst | Copper(1+) iodide; Copper(I) iodide; Cuprous iodide; Cuprous iodide (CuI) | HCID 24350 | — |
| Product | HCID 57634228 | HCID 57634228 | — |
Reaction Steps
The compound was prepared by a method analogous to that described in Preparation 3 from (S)-spiro[1-azabicyclo[2.2.2]octan-3,5′-oxazolidin]-2′-one and 2-bromo-5-phenyl-1,3,4-thiadiazole using 5 equivalents of copper (I) iodide. The title compound (180 mg) was obtained as a yellow solid, m/z 343 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514567B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-d3a9d93e954b493fab15398462492954 |
| Source note | uspto-grants-2009_04 |