HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorobenzenesulfonyl Chloride → HCID 9935267, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorobenzenesulfonyl Chloride | HCID 2734258 | — |
| Reactant | HCID 15512340 | HCID 15512340 | — |
| Reactant | HCID 68969965 | HCID 68969965 | — |
| Product | HCID 9935267 | HCID 9935267 | — |
Reaction Steps
From 0.3 mmol of 2′-aminomethylbiphenyl-2-carboxylic acid 2-(2-pyridyl)-ethylamide (precursor 5d) and 3-fluorophenylsulfonyl chloride, according to the general working procedure 102 mg of 2′-(3-fluorophenylsulfonyl-aminomethyl)biphenyl-2-carboxylic acid 2-(2-pyridyl)ethylamide were obtained; m.p. 123° C. MS (ES+): m/e=490 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514582B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-03166ef36c654448bcd3b75442975828 |
| Source note | uspto-grants-2009_04 |