HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylethylenediamine → HCID 178484251, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylethylenediamine | HCID 8014 | — |
| Reactant | 8-chloro-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one | HCID 3653116 | — |
| Product | HCID 178484251 | HCID 178484251 | 25.3% |
Reaction Steps
8-Chloro-5,10-dihydro-dibenzo[b,e][1,4]diazepine-11-one (25 mg, 0.1 mmol) and N-methylethylenediamine (74 mg, 1.0 mmol) were reacted according to GP4 to give 7.6 mg of the title compound (160FE22). MS (ESI) 301 (MH+). Purity for MH+ (UV/MS) 92/83.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07517871B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-daca8bf5c09846849c3fb44ce3d90e31 |
| Source note | uspto-grants-2009_04 |