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HRID2109965

反应详情

EQUATION

反应方程式

HRID 2109965 的结构方程式

REACTANTS

反应物

2
反应SMILES：CN(CC[N+](C)(C)C)c1ccc([N+](=O)[O-])cc1.COS(=O)(=O)[O-]
HCID18522685

N,N,N-trimethyl-2-[methyl(4-nitrophenyl)-amino]ethanaminium methylsulfate

C13H23N3O6S

反应SMILES：[H][H]
HCID178418361

未命名化合物

PRODUCTS

产物

1
反应SMILES：CN(CC[N+](C)(C)C)c1ccc(N)cc1.COS(=O)(=O)[O-]
HCID86760851

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
反应SMILES：[Pd]
催化剂HCID23938

Palladium

Pd

反应SMILES：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

10 g (28.6 mmol) of the compound from Step 9.2 was dissolved in 80 mL of water and hydrogenated in the presence of 1 g of Pd/C (10%) under 9 bar of hydrogen pressure. After 2 hours, the catalyst was filtered off and the filtrate was evaporated to dryness. This gave 9.3 g (99.6% of the theoretical) of a brown oil.

WORKUP

后处理

  1. filtrationthe catalyst was filtered off
  2. customthe filtrate was evaporated to dryness