Benzenesulfonyl chloride → HCID 57636456, compound

Participants

Reaction Conditions

Reaction Steps

N*3*-Isopropyl-1H-indazole-3,6-diamine (0.036 g, 0.19 mmol) was dissolved in 1 mL pyridine and benzenesulfonyl chloride (0.024 mL, 0.19 mmol) was added. The reaction mixture was heated to 100° C. and stirred for an hour, then cooled and concentrated under reduced pressure. The residue was chromatographed through silica gel (EtOAc/hexanes 0-50%) to give 6.0 mg of N-(3-Isopropylamino-1H-indazol-6-yl)-benzenesulfonamide, MS (M+H)=359.

Provenance & Evidence