HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Allylphenol → Benzoxazines
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Allylphenol | HCID 15624 | — |
| Reactant | Aminopropyltrimethoxysilane | HCID 83756 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Benzoxazines | HCID 17845026 | 94% |
Reaction Steps
This compound was prepared according to the method described in the previous examples using 3-aminopropyltrimethoxysilane (17.9 g, 100 mmole), paraformaldehade (6.3 g, 210 mmole), 2-allyl-phenol (13.4 g, 0.1 mmole), and toluene (200 ml). The final product was obtained as a slightly yellow, mobile liquid. The yield was 94% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07517925B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-07ae610679b74ca0ba892db9663b542a |
| Source note | uspto-grants-2009_04 |