HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → Benzoxazines
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | HCID 69054133 | HCID 69054133 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Benzoxazines | HCID 17845026 | — |
Reaction Steps
The desired benzoxazine was prepared from the reaction of ethylene diamine (0.9 g, 15 mmole), 2-[(trimethoxysilyl)propyl]phenol (7.68 g, 30 mmole, prepared as described in Example 12A), paraformaldehyde (2.1 g, 70 mmole), and toluene (20 ml). The final product was a viscous liquid. The yield was 65% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07517925B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-1fa1298fad824d47a0700ec269f23cea |
| Source note | uspto-grants-2009_04 |