HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → Benzoxazines
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | (3-Aminopropyl)triethoxysilane | HCID 13521 | — |
| Reactant | 1-(4-hydroxyphenyl)-1H-pyrrole-2,5-dione | HCID 81734 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Benzoxazines | HCID 17845026 | 37% |
Reaction Steps
This compound was prepared according to the method used for the previous examples by combining 4-maleimidophenol (18.9 g, 100 mmol), 3-aminopropyltriethoxysilane (22.1 g, 100 mmol), paraformaldehyde (6.3 g, 210 mmol), and toluene (150 mL). The final product was a highly viscous red liquid. The yield was 37%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07517925B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-57b981b4255445acbcd958a0616459f7 |
| Source note | uspto-grants-2009_04 |