Trimethylsilyl iodide → HCID 68838120, compound

Participants

Reaction Steps

To a solution of Example 8B (0.31g, 0.98 mmol) in acetonitrile (0.2 mL) was added iodotrimethylsilane (TMSI) (1 mL, 6.86 mmol). The reaction solution was stirred at room temperature for 4 h. The solution was concentrated in vacuo. Column chromatography on silica (50% ethyl acetate/hexane) afforded the title compound as a white solid (0.28g, 95%).

Provenance & Evidence