HCID 135885194, compound → HCID 136383514, compound

Participants

Reaction Steps

The procedure of Example 91 was followed, except substituting the product from Example 81 with the product from Example 88. The title compound was prepared as a light yellow solid (8 mg, 57%). 1H NMR (300 MHz, DMSO-d6) δ ppm 0.41-0.59 (m, 1H), 0.66 (s, 9H), 0.91-1.08 (m, 1H), 1.74-2.26 (m, 2H), 3.01 (s, 3H), 6.75 (d, J=5.15 Hz, 2H), 7.13 (d, J=5.88 Hz, 2H), 7.32-7.39 (m, 1H), 7.40-7.55 (m, 3H), 7.55-7.68 (m, 1H), 7.75-7.90 (m, 1H), 8.14 (d, J=6.99 Hz, 1H), 9.94 (s, 1H); MS m/z 639.3 (M+H)+.

Provenance & Evidence