Carbon Dioxide → HCID 178527662, compound

HRID 2111499Notes

Reaction equation

HRID 2111499 reaction equation
[CH2:1]([S:6]([OH:9])(=[O:8])=[O:7])[S:2]([OH:5])(=[O:4])=[O:3].C(=O)([O-])[O-].[Ag+2:14].C(=O)=O>O>[CH2:1]([S:6]([O-:9])(=[O:8])=[O:7])[S:2]([O-:5])(=[O:4])=[O:3].[Ag+2:14]

Participants

5

Reactant 3

HCID 280Carbon DioxideHCID 10427Methanedisulfonic acidHCID 178418647HCID 178418647, compound2×

Product 1

HCID 178527662HCID 178527662, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

A 50% solution of methanedisulfonic acid in water (2.5 grams) was diluted in 25 mL of water into which, while stirring, silver carbonate (3.91 grams) was added slowly. The silver carbonate dissolved with effervescence of carbon dioxide. After the reaction was complete remaining insoluble material was removed by filtration and the filtrate was stripped of water and dried under high vacuum at 45° C. to give 4.9 grams of white crystals.

Workup

  1. customwas removed by filtration
  2. customdried under high vacuum at 45° C.

Sources & evidence

ORD record
ord-f0109359157e4020addd10564fe958e8
Source dataset
uspto-grants-2009_04
Patent number
US07521170B2

Reaction notes

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