HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86611351, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 10857231 | HCID 10857231 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86611351 | HCID 86611351 | 98% |
Reaction Steps
A solution of methyl (2E)(4S)-4-[(tert-butoxy)carbonylamino]pent-2-enoate (3.083 g, 13.45 mmol) in 4N hydrogen chloride in dioxane was stirred at room temperature for 1 hour. The volatiles were evaporated to give the title compound (2.2 g, 98%): ES-MS (m/z) 130.3 [M+1]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07521446B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-fb71f71cf68f4074bacf7432d99044ac |
| Source note | uspto-grants-2009_04 |