反应详情

The product of above-mentioned (b) (4.1 g, 18 mmol) was heated under reflux in acetic anhydride (14 ml) for 10 minutes. The reaction solution was poured into ice-cold water, and extracted with chloroform. The organic layer was washed with an aqueous saturated sodium bicarbonate solution and then water, dried and concentrated under reduced pressure to give 1.8 g of the title compound.

1. additionThe reaction solution was poured into ice-cold water
2. extractionextracted with chloroform
3. washThe organic layer was washed with an aqueous saturated sodium bicarbonate solution
4. dry with materialwater, dried
5. concentrationconcentrated under reduced pressure