HCID 23151368, compound → HCID 23151345, compound

HRID 2111835Notes

Reaction equation

HRID 2111835 reaction equation
[CH:1]1([N:6]2[CH2:11][CH2:10][CH:9]([O:12][C:13]3[CH:18]=[CH:17][C:16]([N+:19]([O-])=O)=[CH:15][CH:14]=3)[CH2:8][CH2:7]2)[CH2:5][CH2:4][CH2:3][CH2:2]1>CO>[CH:1]1([N:6]2[CH2:11][CH2:10][CH:9]([O:12][C:13]3[CH:14]=[CH:15][C:16]([NH2:19])=[CH:17][CH:18]=3)[CH2:8][CH2:7]2)[CH2:2][CH2:3][CH2:4][CH2:5]1

Participants

3

Reactant 1

HCID 23151368HCID 23151368, compound

Product 1

HCID 23151345HCID 23151345, compoundYield 86%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

1-cyclopentyl-4-(4-nitrophenoxy)piperidine (1.30 g) was dissolved in methanol, and the target compound (1.0 g, 86%) was obtained as a light brown solid by catalytic reduction using a palladium charcoal catalyst.

Sources & evidence

ORD record
ord-59cb97d0316040348d2b67eef4de21c5
Source dataset
uspto-grants-2009_04
Patent number
US07521455B2

Reaction notes

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