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HRID2111859

反应详情

EQUATION

反应方程式

HRID 2111859 的结构方程式

REACTANTS

反应物

2
结构：Br.BrCCCN1CCCC1
HCID20135920

1-(3-Bromopropyl)pyrrolidine--hydrogen bromide (1/1)

C7H15Br2N

结构：COc1cc2c(=O)n(-c3ccc(O)cc3)c(C)nc2cn1
HCID23151204

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc2c(=O)n(-c3ccc(OCCCN4CCCC4)cc3)c(C)nc2cn1
HCID23151361

未命名化合物

PROCEDURE

实验过程

The title compound was synthesized as a white solid (m.p.:123-126° C.) by the method according to Example 63, using 3-(4-hydroxyphenyl)-6-methoxy-2-methylpyrido[3,4-d]pyrimidin-4(3H)-one synthesized in Example 197 and 1-(3-bromopropyl)pyrrolidine hydrobromide as starting materials, followed by recrystallization (ethyl acetate/diethyl ether).

WORKUP

后处理

  1. customfollowed by recrystallization (ethyl acetate/diethyl ether)