Ammonia → HCID 86608932, compound

Participants

Reaction Steps

To the product from Step 8 is added 7N NH3 in MeOH and the mixture is stirred at ambient temperature until deacetylation is sufficiently complete as determined by TLC. The mixture is concentrated in vacuo and the crude material is taken up and purified by Phenomenex-C18 reverse phase HPLC (Buffer A=H2O, Buffer B=acetonitrile) to afford the title compound.

Provenance & Evidence