huagongshe.com
HRID2112446

反应详情

EQUATION

反应方程式

HRID 2112446 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc(S(=O)(=O)Cl)cc1
HCID7401

4-Methoxybenzenesulphonyl chloride

C7H7ClO3S

结构：CC(C)(C)OC(=O)N1CCN(c2cccc3[nH]ccc23)CC1
HCID22015386

tert-Butyl 4-(1H-indol-4-yl)piperazine-1-carboxylate

C17H23N3O2

PRODUCTS

生成物

1
结构：COc1ccc(S(=O)(=O)n2ccc3c(N4CCNCC4)cccc32)cc1.Cl
HCID10294853

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(4-boc-piperazinyl)-indole and 4-methoxyphenylsulfonyl chloride according to Method 3: 1H NMR (270 MHz, DMSO-d6) δ 9.07 (br, 1H), 7.90 (d, J=8 Hz, 2H), 7.78 (d, J=5 Hz, 1H), 7.61 (d, J=8 Hz, 1H), 7.25 (t, J=8 Hz, 1H), 7.09 (d, J=8 Hz, 2H), 6.92 (d, J=8 Hz, 1H), 6.68 (d, J=8 Hz, 1H), 3.79 (s, 3H), 3.24 (m, 8H); MS (ESI+) for m/z 371 (M+H)+.