HRID2112447

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID2734273

2,4-Difluorobenzenesulfonyl chloride

C6H3ClF2O2S

结构：CC(C)(C)OC(=O)N1CCN(c2cccc3[nH]ccc23)CC1

HCID22015386

tert-Butyl 4-(1H-indol-4-yl)piperazine-1-carboxylate

C17H23N3O2

PRODUCTS

生成物

结构：Cl.O=S(=O)(c1ccc(F)cc1F)n1ccc2c(N3CCNCC3)cccc21

HCID10201828

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(4-boc-piperazinyl)-indole and 2,4-di-fluorophenylsulfonylchloride according to Method 3: 1H NMR (270 MHz, DMSO-d6) δ 9.41 (br, 1H), 8.24 (m, 1H), 7.75 (m, 1H), 7.58 (m, 1H), 7.47-7.33 (m, 2H), 7.23 (t, J=8 Hz, 1H), 6.99 (d, J=5 Hz, 1H), 6.70 (d, J=8 Hz, 1H), 3.25 (m, 8H). MS (ESI+) for m/z 378 (M+H)+.