Sodium Hydroxide → HCID 22593766, compound

HRID 2112687Notes

Reaction equation

HRID 2112687 reaction equation
[OH-].[Na+].[CH3:3][NH:4][C:5]([C:7]1[CH:16]=[CH:15][C:14]2[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=2)[C:8]=1[CH3:17])=O.CNC(C1CC2C(C=1C)=CC=CC=2)=O>>[CH3:17][C:8]1[C:9]2[C:14](=[CH:13][CH:12]=[CH:11][CH:10]=2)[CH:15]=[CH:16][C:7]=1[CH2:5][NH:4][CH3:3]

Participants

4

Reactant 3

HCID 14798Sodium HydroxideHCID 17930140HCID 17930140, compoundHCID 22593706HCID 22593706, compound

Product 1

HCID 22593766HCID 22593766, compoundYield 36%

Procedure

According to the procedure of Preparation 20 (b), except substituting N,1-dimethylnaphthalene-2-carboxamide (0.3 g, 1.5 mmole) for the N,3-dimethylindene-2-carboxamide, the title compound (0.1 g, 36%) was prepared as a colorless oil: MS (ES) m/e 186 (M+H)+.

Sources & evidence

ORD record
ord-ce50c78facaf4d70835c291fc603d715
Source dataset
uspto-grants-2009_04
Patent number
US07524843B2

Reaction notes

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