HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Nitroresorcinol → 2-Aminoresorcinol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Nitroresorcinol | HCID 11760 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-Aminoresorcinol | HCID 69451 | 99.3% |
Reaction Steps
A mixture of 2-nitrobenzene-1,3-diol (5 g, 32.2 mmol) and 10% Pd on charcoal (230 mg) in ethanol (100 ml) were hydrogenated with H2 at atmospheric pressure overnight. The reaction mixture was filtered through celite. Ethanol was removed by evaporation to yield the subtitled compound (4 g, 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07524856B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-061c4bc540db408bbe7e67540094be05 |
| Source note | uspto-grants-2009_04 |