Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethyl isocyanate | HCID 8022 | — |
| Reactant | Di-n-butyl diacetoxy tin | HCID 9798523 | — |
| Reactant | HCID 68835872 | HCID 68835872 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 68839697 | HCID 68839697 | — |
Reaction Steps
A suspension of the product of Step 3 in toluene (20 mL) containing dibutyltin diacetate (0.1 mL) and ethyl isocyanate (0.2 mL) was heated to 110° C. for 48 h. The suspension was cooled and the precipitate was filtered and washed with toluene to give the tile compound as a solid; m.p. 318-321°. ACPI-MS Found: [M+H]+=365.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07524860B2 |
|---|
| Source dataset | uspto-grants-2009_04 |
|---|
| ORD ID | ord-acf72efae1b44a9fa98a900a6b50c2b7 |
|---|
| Source note | uspto-grants-2009_04 |
|---|
