HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2H-1,3-benzodioxol-5-yl)boronic acid → 6-(4-Benzo[1,3]dioxol-5-yl-phenoxymethyl)-pyridine-2-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2H-1,3-benzodioxol-5-yl)boronic acid | HCID 2734371 | — |
| Reactant | 6-(4-Iodo-phenoxymethyl)-pyridine-2-carboxylic acid ethyl ester | HCID 57643352 | — |
| Product | 6-(4-Benzo[1,3]dioxol-5-yl-phenoxymethyl)-pyridine-2-carboxylic acid | HCID 11501161 | — |
Reaction Steps
6-(4-Benzo[1,3]dioxol-5-yl-phenoxymethyl)-pyridine-2-carboxylic acid was prepared using general procedure 3 from 6-(4-iodo-phenoxymethyl)-pyridine-2-carboxylic acid ethyl ester (of Intermediate 3) and 3,4-methylenedioxybenzeneboronic acid (ASDI Incorporated, Newark, Del.). Mass spectrum MH+=350.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07524870B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-33a1f2b00c4f4ba0afd6a3d0dedc0097 |
| Source note | uspto-grants-2009_04 |