HCID 11280704, compound → HCID 44339399, compound

HRID 2113053Notes

Reaction equation

HRID 2113053 reaction equation
[Cl:1][C:2]1[CH:24]=[C:23]([F:25])[CH:22]=[CH:21][C:3]=1[CH2:4][S:5]([NH:8][C:9]1[C:10](=[O:20])[N:11]([CH2:16][C:17](O)=[O:18])[C:12]([CH3:15])=[CH:13][CH:14]=1)(=[O:7])=[O:6].Br.Br.[S:28]1[C:32]2[CH2:33][CH:34]([NH2:37])[CH2:35][CH2:36][C:31]=2[N:30]=[C:29]1[NH2:38]>>[NH2:38][C:29]1[S:28][C:32]2[CH2:33][CH:34]([NH:37][C:17](=[O:18])[CH2:16][N:11]3[C:12]([CH3:15])=[CH:13][CH:14]=[C:9]([NH:8][S:5]([CH2:4][C:3]4[CH:21]=[CH:22][C:23]([F:25])=[CH:24][C:2]=4[Cl:1])(=[O:6])=[O:7])[C:10]3=[O:20])[CH2:35][CH2:36][C:31]=2[N:30]=1

Participants

3

Reactant 2

HCID 11280704HCID 11280704, compoundHCID 136706894,5,6,7-Tetrahydro-benzothiazole-2,6-diamine dihydrobromide

Product 1

HCID 44339399HCID 44339399, compound

Procedure

The title compound was prepared from 2-[3-{[(2-chloro-4 -fluorobenzyl)sulfonyl]amino}-6-methyl-2-oxo-1(2H)-pyridinyl]acetic acid and 4,5,6,7-tetrahydro-1,3-benzothiazol-2,6-diamine dihydrobromide using the procedure of EXAMPLE 1 (STEP 6), and was obtained as a white solid compound.

Workup

  1. customwas obtained as a white solid compound

Sources & evidence

ORD record
ord-7740b2b01b764f5cbac46b7925556dc4
Source dataset
uspto-grants-2009_04
Patent number
US07524871B2

Reaction notes

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