HuagongsheHuagongshe Chemistry Print Report · For research reference only
Borohydride → 4-Methoxy-3-(4-methoxyphenyl)benzyl alcohol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Borohydride | HCID 28123 | — |
| Reactant | 6,4'-Dimethoxybiphenyl-3-carbaldehyde | HCID 22391191 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-Methoxy-3-(4-methoxyphenyl)benzyl alcohol | HCID 68841639 | 87.2% |
Reaction Steps
A solution of 4-methoxy-3-(4-methoxyphenyl)benzenecarboxaldehyde (1 g, 4.13 mmol) in methanol (12 mL) was treated with polymer-supported borohydride (10.3 mmol) and the mixture shaken for 16 hours. The resin was then filtered and the filtrate concentrated under reduced pressure to afford 0.88 g of title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07524873B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-a04e692fa7c14bc6ba04c1ac262bf2c6 |
| Source note | uspto-grants-2009_04 |