HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butanoic acid, 4-chloro-3-hydroxy-, ethyl ester → Ethyl 4-chloroacetoacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butanoic acid, 4-chloro-3-hydroxy-, ethyl ester | HCID 4377704 | — |
| Reactant | 1066-35-9 | HCID 6327132 | — |
| Product | Ethyl 4-chloroacetoacetate | HCID 69484 | — |
Reaction Steps
The quantitation of ethyl 4-chloro-3-hydroxybutyrate was carried out by gas chromatography. Thus, using a glass column (ID 3 mm×1 m) packed with PEG-20M Chromosorb WAW DMCS 10%, 80/100 mesh (product of GL Sciences Inc.), chromatography was carried out at 150° C. The detection was made by FID.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07432095B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-1c63baaa7b784e589ea1319894e1fcf4 |
| Source note | uspto-grants-2008_10 |