HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 68406810, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Fluoro-5-methoxybenzonitrile | HCID 2774546 | — |
| Reactant | HCID 178418800 | HCID 178418800 | — |
| Product | HCID 68406810 | HCID 68406810 | 72% |
Reaction Steps
In analogy to example 5a, 2-fluoro-5-methoxy-benzonitrile was reacted with 4-methylimidazole and potassium carbonate for 48 h at 100° C. After aqueous workup and crystallization from Ethyl acetate/diisopropylether the title compound was obtained as a white solid (yield: 72%). MS: m/e=214.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07432256B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-517c05b2479946dc8d4cc57a3b81628e |
| Source note | uspto-grants-2008_10 |