HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl(methylene)ammounium iodide → HCID 67549738, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl(methylene)ammounium iodide | HCID 2724133 | — |
| Reactant | HCID 68406810 | HCID 68406810 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67549738 | HCID 67549738 | 83% |
Reaction Steps
In analogy to example 5b, 5-methoxy-2-(4-methyl-imidazol-1-yl)-benzonitrile was reacted with Eschenmoser's salt in DMF for 16 h at 70° C. Evaporation of the solvent, aqueous workup and chromatography afforded the title compound as an oil (yield: 83%). MS: m/e=271.4 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07432256B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-b55bfc4ddda74493b8792d91965a3fbf |
| Source note | uspto-grants-2008_10 |