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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2113478Generated: October 27, 2026

tert-Butyl carbazate → tert-butyl N'-(quinolin-2-yl)methylene-hydrazinecarboxylate

https://huagongshe.com/reaction/2113478

Reaction equation

Participants

RoleNameHCIDCharge
Reactanttert-Butyl carbazateHCID 70091—
Reactant2-QuinolinecarboxaldehydeHCID 79619—
SolventEthanolHCID 702—
Producttert-butyl N'-(quinolin-2-yl)methylene-hydrazinecarboxylateHCID 69201455—

Reaction Steps

A solution of 10.70 g 2-quinolinecarboxaldehyde and 9.00 g tert-butyl hydrazinecarboxylate in 200 ml of ethanol is refluxed for 2 h with stirring. Then the solution is evaporated to dryness and the residue is triturated with diisopropylether, separated off and dried at 50° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07432262B2
Source datasetuspto-grants-2008_10
ORD IDord-1856801b857e41b486abb4661ce3c0d9
Source noteuspto-grants-2008_10