HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 69245143, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Chloro-5-phenyloxazole | HCID 10997626 | — |
| Reactant | 4-[3-(Trifluoromethyl)phenyl]-1-piperazinebutanamine | HCID 11162411 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 69245143 | HCID 69245143 | — |
Reaction Steps
A solution of 35 mg (0.2 mmol) of 2-chloro-5-phenyloxazole in 0.5 mL of tetrahydrofuran is added, at 0° C., to a solution of 62 mg (0.2 mmol) of 4-[4-(3-trifluoromethylphenyl)piperazine-1-yl]butylamine (Example 3, step b) and 20 mg (0.2 mmol) of triethylamine in 0.2 mL of tetrahydrofuran. The mixture is stirred overnight under argon.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07432269B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-27bc0977600f44269f43b8ba09e81b56 |
| Source note | uspto-grants-2008_10 |