HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-(aminomethyl)benzoate → HCID 69146688, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-(aminomethyl)benzoate | HCID 571728 | — |
| Reactant | 3-Chloro-4-phenylfuran-2,5-dione | HCID 23447195 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 69146688 | HCID 69146688 | — |
Reaction Steps
A solution of 3-chloro-4-phenylfuran-2,5-dione (0.24 mmol, 50 mg) and methyl 4-(aminomethyl)benzoate (0.24 mmol, 40 mg) in glacial acetic acid (1 mL) was heated in a microwave reactor at 120° C. for two min. After cooling, the solvent was evaporated at reduced pressure. The crude product was used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07432288B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-5b0de6ea414f41ef9965ccda6f799af8 |
| Source note | uspto-grants-2008_10 |