HCID 15490830, compound → HCID 22243668, compound

Participants

Reaction Steps

A suspension of 1.0 eq of 89 and 0.1 wt/wt eq of 10% Pd on carbon in 35 mL of EtOH was hydrogenated under 50 psi of H2 for 30 min, until consumption of H2 ceased. The reaction mixture was filtered through Celite. The filtrate was concentrated by rotary evaporation. The crude material was dried under vacuum to give acid 90.

Provenance & Evidence