HCID 59809555, compound → HCID 11538047, compound

HRID 2114503Notes

Reaction equation

HRID 2114503 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][CH:9]2[CH2:14][CH2:13][N:12]([CH3:15])[CH2:11][CH2:10]2)=[C:4]([S:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=2Br)[CH:3]=1.C(OC(N1CCC(NC2C=CC(C#N)=CC=2OC2C=CC=CC=2Br)CC1)=O)(C)(C)C>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]2[N:8]([CH:9]3[CH2:14][CH2:13][N:12]([CH3:15])[CH2:11][CH2:10]3)[C:22]3[C:17]([S:16][C:4]=2[CH:3]=1)=[CH:18][CH:19]=[CH:20][CH:21]=3

Participants

3

Reactant 2

HCID 59809555HCID 59809555, compoundHCID 59809564HCID 59809564, compound2×

Product 1

HCID 11538047HCID 11538047, compound

Procedure

Using an adaptation of the method described in Procedure 4, substituting [4-bromo-2-(2-bromophenylsulfanyl)-phenyl]-(1-methyl-piperidin-4-yl)-amine, 3e for 4-[2-(2-bromophenoxy)-4-cyanophenylamino]-piperidine-1-carboxylic acid tert-butyl ester, 3a, the title compound 3-bromo-10-(1-methylpiperidin-4-yl)-10H-phenothiazine, 4e was obtained. MS m/z (MH+) 375.1/377.1.

Sources & evidence

ORD record
ord-547f8ce44d9749d7a8b5875ca54c60a4
Source dataset
uspto-grants-2008_10
Patent number
US07432257B2

Reaction notes

Loading…