Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 9953250 | HCID 9953250 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 9843570 | HCID 9843570 | 10.1% |
Reaction Steps
To a solution of 1-(4-bromobenzyl)-6-methoxy-2-phenyl-1,2,3,4-tetrahydroisoquinoline (0.10 g, 0.25 mmol) in CH2Cl2 (15 mL) at 0° C. under nitrogen was added boron tribromide (1.47 mL, 1.47 mmol). The reaction was allowed to reach RT. After 8 hours, the reaction was poured into water (10 mL) and neutralized with saturated sodium bicarbonate. Additional CH2Cl2 (25 mL) was added, the organic layer was separated, dried over MgSO4, filtered and concentrated. The residue was then chromatographed (SiO2, 2:1, hexanes/ethyl acetate) to provide the title compound (0.010 g, 10% yield): 1H NMR (CDCl3) 7.33 (d, 2H), 7.24 (dd, 2H), 6.97 (d, 1H), 6.88 (d, 2H), 6.80 (d, 2H), 6.75 (dd, 2H), 6.66 (m, 1H), 6.27 (s, 1H), 4.78 (t, 1H), 3.53 (m 2H), 3.13 (dd, 1H), 2.96 (m, 2H), 2.62 (m, 1H); ES-MS (m/z) 392 [M−H]−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07435729B2 |
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| Source dataset | uspto-grants-2008_10 |
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| ORD ID | ord-1b5eb5f43164438d9789c7f2b8c6e485 |
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| Source note | uspto-grants-2008_10 |
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