HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 54711997, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 54712022 | HCID 54712022 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 54711997 | HCID 54711997 | — |
Reaction Steps
The product of Step 1 was treated with a mixture HCl 1N/THF for 1 hour at 40° C. Organics were removed in vacuo and residue extracted in DCM, dried over Na2SO4 and concentrated to give the title compound as a foam which was immediately reacted in the following reductive amination.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435734B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-910071db49ab489b883b441226899495 |
| Source note | uspto-grants-2008_10 |