HCID 69147861, compound → HCID 69316437, compound

HRID 2114843Notes

Reaction equation

HRID 2114843 reaction equation
[CH2:1]([N:3]1[C:8](=[O:9])[CH2:7][N:6](C(OCC2C=CC=CC=2)=O)[CH2:5][C:4]1([CH3:21])[CH3:20])[CH3:2]>[Pd]>[CH2:1]([N:3]1[C:4]([CH3:21])([CH3:20])[CH2:5][NH:6][CH2:7][C:8]1=[O:9])[CH3:2]

Participants

3

Reactant 1

HCID 69147861HCID 69147861, compound

Product 1

HCID 69316437HCID 69316437, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

The compound was prepared from benzyl 4-ethyl-3,3-dimethyl-5-oxopiperazine-1-carboxylate using a procedure similar to that described in Example 66, Step 6, except that Degussa type 10% palladium on carbon was used as the catalyst, and the additional filtration with toluene was unnecessary.

Workup

  1. filtrationthe additional filtration with toluene

Sources & evidence

ORD record
ord-8b83e1e297c844d9be0886c2d0d12f91
Source dataset
uspto-grants-2008_10
Patent number
US07435735B2

Reaction notes

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