3-Chlorothiophene-2-carbonyl chloride → HCID 22147903, compound

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Reaction Steps

The title compound was prepared from 5-nitro-thiazole-2-amidoxime (17.2 mg, 0.0914 mmol) and 3-chloro-thiophene-2-carbonyl chloride (16.4 mg, 0.0905 mmol) similar to Example 16, and yielded 6.7 mg (23%) of yellow solid. 1H NMR (CDCl3): 8.74 (s, 1H), 7.70 (d, J=5.22 Hz, 1H), 7.18 (d, J=5.22 Hz, 1H).

Provenance & Evidence