2-(3-nitroanilino)-2-oxoacetic acid → HCID 69099830, compound

HRID 2114974Notes

Reaction equation

HRID 2114974 reaction equation
[F:1][C:2]1[CH:14]=[CH:13][C:5]([CH2:6][CH:7]2[CH2:12][CH2:11][NH:10][CH2:9][CH2:8]2)=[CH:4][CH:3]=1.[N+:15]([C:18]1[CH:19]=[C:20]([NH:24][C:25](=[O:29])[C:26](O)=[O:27])[CH:21]=[CH:22][CH:23]=1)([O-:17])=[O:16]>C(OCC)C>[F:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:6][CH:7]2[CH2:8][CH2:9][N:10]([C:26](=[O:27])[C:25]([NH:24][C:20]3[CH:21]=[CH:22][CH:23]=[C:18]([N+:15]([O-:17])=[O:16])[CH:19]=3)=[O:29])[CH2:11][CH2:12]2)=[CH:13][CH:14]=1

Participants

4

Reactant 2

HCID 2355122-(3-nitroanilino)-2-oxoacetic acidHCID 36998414-(4-Fluoro-benzyl)-piperidine

Product 1

HCID 69099830HCID 69099830, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

The title compound is prepared from 4-(4-fluoro-benzyl)-piperidine and N-(3-nitro-phenyl)-oxalamic acid (Example 10a according to the method described in Example 2. Melting Point: 135-138° C. (diethylether)

Sources & evidence

ORD record
ord-a477cb3e70174e7e80fb9ac5d9ecb3c0
Source dataset
uspto-grants-2008_10
Patent number
US07435744B2

Reaction notes

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