Sulfanilamide → HCID 69101225, compound

HRID 2115068Notes

Reaction equation

HRID 2115068 reaction equation
[S:1]([NH2:11])(=[O:10])([C:3]1[CH:8]=[CH:7][C:6]([NH2:9])=[CH:5][CH:4]=1)=[O:2].[F:12][C:13]1[CH:30]=[CH:29][C:16]([CH2:17][CH:18]2[CH2:23][CH2:22][N:21]([C:24](=[O:28])[C:25](O)=[O:26])[CH2:20][CH2:19]2)=[CH:15][CH:14]=1>C(OCC)C>[F:12][C:13]1[CH:30]=[CH:29][C:16]([CH2:17][CH:18]2[CH2:19][CH2:20][N:21]([C:24](=[O:28])[C:25]([NH:9][C:6]3[CH:5]=[CH:4][C:3]([S:1](=[O:10])(=[O:2])[NH2:11])=[CH:8][CH:7]=3)=[O:26])[CH2:22][CH2:23]2)=[CH:15][CH:14]=1

Participants

4

Reactant 2

HCID 5333SulfanilamideHCID 51342220[4-(4-Fluorobenzyl)piperidin-1-yl](oxo)acetic acid

Product 1

HCID 69101225HCID 69101225, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

The title compound is prepared from sulfanilamide (Aldrich) and [4-(4-fluoro-benzyl)-piperidin-1-yl]oxo-acetic-acid (Example 1b) according to the method described in Example 1c. Melting Point: 201-203° C. (diethylether)

Sources & evidence

ORD record
ord-496561c3511c49dfa4e22de18e3b3df4
Source dataset
uspto-grants-2008_10
Patent number
US07435744B2

Reaction notes

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