HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Benzyloxy)piperidine → 2-(4-Benzyloxy-piperidin-1-yl)-N-(3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-7-yl)-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Benzyloxy)piperidine | HCID 3157460 | — |
| Reactant | 2-chloro-N-(3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-7-yl)-acetamide | HCID 24298282 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-(4-Benzyloxy-piperidin-1-yl)-N-(3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-7-yl)-acetamide | HCID 69099892 | — |
Reaction Steps
The title compound is prepared from 2-chloro-N-(3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-7-yl)-acetamide (Example 153a) and 4-benzyloxy-piperidine according to the method described in Example 142b. Melting Point: 238-240° C. (diethylether)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435744B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-85d4e1e12ede48f984d55fbdbc6177ad |
| Source note | uspto-grants-2008_10 |