Acetaldehyde → HCID 69100083, compound
Reaction equation
[CH:1](=[O:3])[CH3:2].[NH2:4][C:5]1[CH:14]=[CH:13][C:8]2[NH:9][C:10](=[O:12])[O:11][C:7]=2[CH:6]=1.[CH2:15]([O:17][CH2:18][CH3:19])[CH3:16]>>[O:3]=[C:1]([N:9]1[CH2:8][CH2:7][CH:15]([O:17][C:18]2[CH:13]=[CH:14][CH:5]=[CH:6][CH:19]=2)[CH2:16][CH2:10]1)[CH2:2][NH:4][C:5]1[CH:14]=[CH:13][C:8]2[NH:9][C:10](=[O:12])[O:11][C:7]=2[CH:6]=1Participants
4
Procedure
The title compound is prepared from 2-chloro-1-(4-phenoxy)-piperidin-1-yl]-ethanone and 6-amino-3H-benzoxazol-2-one according to the method described in Example 206. Melting Point:220-223° C. (diethylether)
Sources & evidence
- ORD record
- ord-735d135b02724d81863315aac9b41c3a
- Source dataset
- uspto-grants-2008_10
- Patent number
- US07435744B2
Reaction notes
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