HCID 10236835, compound → HCID 10171533, compound

HRID 2115263Notes

Reaction equation

HRID 2115263 reaction equation
C(OC([C:6]1[S:7][C:8](C(O)=O)=[C:9]2[C:15]=1[C:14]1[CH:16]=[CH:17][CH:18]=[CH:19][C:13]=1[S:12][C:11]1[CH:20]=[CH:21][CH:22]=[CH:23][C:10]2=1)=O)C.C(OC(C1SC=C2C=1C1C=CC=CC=1SC1C=CC=CC2=1)=O)C>>[CH:8]1[S:7][CH:6]=[C:15]2[C:9]=1[C:10]1[CH:23]=[CH:22][CH:21]=[CH:20][C:11]=1[S:12][C:13]1[CH:19]=[CH:18][CH:17]=[CH:16][C:14]2=1

Participants

3

Reactant 2

HCID 10236835HCID 10236835, compoundHCID 10237387HCID 10237387, compound

Product 1

HCID 10171533HCID 10171533, compound

Procedure

According to the process of Example 4, starting from dicarboxylate 4 there were prepared compounds 8 and 11. The mixture of the compounds was separated by chromatography on a column to give both products in crystal form.

Workup

  1. additionThe mixture of the compounds
  2. customwas separated by chromatography on a column
  3. customto give both products in crystal form

Sources & evidence

ORD record
ord-de2185b2ad60485cabe5fef87a242dd2
Source dataset
uspto-grants-2008_10
Patent number
US07435834B2

Reaction notes

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