HCID 10308260, compound → HCID 10125881, compound
Reaction equation
[C:1]1([CH2:19][OH:20])[S:2][CH:3]=[C:4]2[C:10]=1[C:9]1[CH:11]=[CH:12][CH:13]=[CH:14][C:8]=1[O:7][C:6]1[CH:15]=[CH:16][CH:17]=[CH:18][C:5]2=1.Cl.Cl[CH2:23][CH2:24][CH2:25][NH2:26]>>[C:1]1([CH2:19][O:20][CH2:23][CH2:24][CH2:25][NH2:26])[S:2][CH:3]=[C:4]2[C:10]=1[C:9]1[CH:11]=[CH:12][CH:13]=[CH:14][C:8]=1[O:7][C:6]1[CH:15]=[CH:16][CH:17]=[CH:18][C:5]2=1Participants
3
Procedure
Starting from the alcohol 12 (0.25 mmole) and 3-chloropropylamine-hydrochloride (2.5 mmoles), an oily product was obtained.
Workup
- customan oily product was obtained
Sources & evidence
- ORD record
- ord-9778ea103e5c4a1aab75f9fb9d47c132
- Source dataset
- uspto-grants-2008_10
- Patent number
- US07435834B2
Reaction notes
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