HCID 10308545, compound → HCID 10126499, compound
Reaction equation
[Cl:1][C:2]1[CH:21]=[CH:20][C:5]2[O:6][C:7]3[CH:19]=[CH:18][CH:17]=[CH:16][C:8]=3[C:9]3[C:13]([C:4]=2[CH:3]=1)=[CH:12][S:11][C:10]=3[CH2:14][OH:15].Cl.[CH3:23][N:24]([CH3:28])[CH2:25][CH2:26]Cl>>[Cl:1][C:2]1[CH:21]=[CH:20][C:5]2[O:6][C:7]3[CH:19]=[CH:18][CH:17]=[CH:16][C:8]=3[C:9]3[C:13]([C:4]=2[CH:3]=1)=[CH:12][S:11][C:10]=3[CH2:14][O:15][CH2:26][CH2:25][N:24]([CH3:28])[CH3:23]Participants
3
Procedure
Starting from the alcohol 13 (0.29 mmole) and 2-dimethylaminoethylchloride-hydrochloride (2.9 mmoles), an oily product was obtained.
Workup
- customan oily product was obtained
Sources & evidence
- ORD record
- ord-ac2bcbdf690743ddb28c875649e8c989
- Source dataset
- uspto-grants-2008_10
- Patent number
- US07435834B2
Reaction notes
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