HCID 10308546, compound → HCID 10126317, compound
Reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[O:14][C:13]3[CH:15]=[CH:16][CH:17]=[CH:18][C:12]=3[C:11]3[C:7](=[C:8]([CH2:19][OH:20])[S:9][CH:10]=3)[C:6]=2[CH:21]=1.Cl.Cl[CH2:24][CH2:25][CH2:26][NH2:27]>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[O:14][C:13]3[CH:15]=[CH:16][CH:17]=[CH:18][C:12]=3[C:11]3[C:7](=[C:8]([CH2:19][O:20][CH2:24][CH2:25][CH2:26][NH2:27])[S:9][CH:10]=3)[C:6]=2[CH:21]=1Participants
3
Procedure
Starting from the alcohol 14 (0.18 mmole) and 3-chloropropylamine-hydrochloride (1.8 mmoles), an oily product was obtained.
Workup
- customan oily product was obtained
Sources & evidence
- ORD record
- ord-0390d87edab74cb7a6d41ef3df1a356d
- Source dataset
- uspto-grants-2008_10
- Patent number
- US07435834B2
Reaction notes
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