HCID 10149515, compound → HCID 11474095, compound

HRID 2115273Notes

Reaction equation

HRID 2115273 reaction equation
[C:1]1([CH2:19][OH:20])[S:2][CH:3]=[C:4]2[C:10]=1[C:9]1[CH:11]=[CH:12][CH:13]=[CH:14][C:8]=1[S:7][C:6]1[CH:15]=[CH:16][CH:17]=[CH:18][C:5]2=1.Cl.[CH3:22][N:23]([CH3:27])[CH2:24][CH2:25]Cl>>[C:1]1([CH2:19][O:20][CH2:25][CH2:24][N:23]([CH3:27])[CH3:22])[S:2][CH:3]=[C:4]2[C:10]=1[C:9]1[CH:11]=[CH:12][CH:13]=[CH:14][C:8]=1[S:7][C:6]1[CH:15]=[CH:16][CH:17]=[CH:18][C:5]2=1

Participants

3

Reactant 2

HCID 10149515HCID 10149515, compoundHCID 11636816N,N-Dimethylaminoethyl chloride hydrochloride

Product 1

HCID 11474095HCID 11474095, compound

Procedure

Starting from the alcohol 15 (0.67 mmole) and 2-dimethylaminoethylchloride-hydrochloride (6.7 mmoles), an oily product was obtained;

Workup

  1. customan oily product was obtained

Sources & evidence

ORD record
ord-5716ecacba6e4d8a92eb9d5bb5c153f9
Source dataset
uspto-grants-2008_10
Patent number
US07435834B2

Reaction notes

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