Ethylamine → HCID 58978364, compound

HRID 2115322Notes

Reaction equation

HRID 2115322 reaction equation
[CH2:1]([NH2:3])[CH3:2].[CH2:4]([NH:6][C:7]([C:9]1[CH:14]=[CH:13][CH:12]=[C:11](Br)[N:10]=1)=[O:8])[CH3:5]>C(O)C.O>[CH2:4]([NH:6][C:7]([C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([NH:3][CH2:1][CH3:2])[N:10]=1)=[O:8])[CH3:5]

Participants

4

Reactant 2

HCID 6341EthylamineHCID 18668644HCID 18668644, compound

Product 1

HCID 58978364HCID 58978364, compound

Reagents, catalysts & solvents 1

HCID 19096565Water ethanolSolvent

Procedure

prepared by reaction of ethylamine with 6-bromo-pyridine-2-carboxylic acid ethylamide; in contrast to the general procedure the reaction was carried out by heating a solution of the starting materials in ethanol/water for 72 h at 100° C. in an autoclave

Sources & evidence

ORD record
ord-a8b2765bc27f4141adb45a62e8279df8
Source dataset
uspto-grants-2008_10
Patent number
US07435815B2

Reaction notes

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