HRID2115882

反应详情

EQUATION

反应方程式

HRID 2115882 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 1-methyl-4-[(4-nitrophenyl)acetyl]piperazine(1.5 g, 5.70 mmol) in EtOH (30 mL) was reduced over palladium/charcoal (10% wt, 50% wet, 150 mg) with hydrogen under atmospheric pressure and RT for 18 h. The catalyst was separated by filtration through Celiteo and the solvent evaporated to the title compound as a brown oil, 1.12 g.

WORKUP

后处理

  1. customThe catalyst was separated by filtration through Celiteo
  2. customthe solvent evaporated to the title compound as a brown oil, 1.12 g