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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2116079Generated: October 31, 2026

Benzyl chloroformate → HCID 91234359, compound

https://huagongshe.com/reaction/2116079

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzyl chloroformateHCID 10387—
ReactantDiisopropylethylamineHCID 81531—
ReactantHCID 68968198HCID 68968198—
ProductHCID 91234359HCID 9123435996.7%

Reaction Steps

Treatment of (±)-benzyl[7-(4-chloro-2-methylphenyl)-2,3-dihydro-1-benzofuran-2-yl]methanamine (0.979 g, 3.15 mmol) with diisopropylethylamine (0.612 g, 4.73 mmol) and benzyl chloroformate (0.646 g, 3.79 mmol) generally according to the procedure described for Intermediate 12 provided 1.2 g (96%) of (±)-benzyl[7-(4-chloro-2-methylphenyl)-2,3-dihydro-1-benzofuran-2-yl]carbamate as a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07435837B2
Source datasetuspto-grants-2008_10
ORD IDord-9151d5a75868466bbe463e8712ab4a49
Source noteuspto-grants-2008_10