Trimethylsilyl iodide → HCID 11413493, compound

Participants

Reaction Steps

The title compound was prepared (0.17 g, 78%) following the general procedure of Example 129 as a yellow solid, hydrochloride salt from (+)-benzyl {[7-pyridin-3-yl-2,3-dihydro-1-benzofuran-2-yl]methyl}carbamate (0.30 g, 0.832 mmol) and trimethylsilyl iodide (0.66 g, 3.33 mmol). [α]D25=+27.2 (c 10.0 in methanol); mp 168-171° C.

Provenance & Evidence